Past Abstracts - 1996 part 1

Technical presentations April 1996

1. "Downhole injection of raw sea water", Dr Roger Francis, Weir Materials

Injection of raw sea water is being considered for a number of offshore projects where space/weight is paramount e.g. floating production platforms. 

The corrosion problems were outlined both for raw water injection and re-injection of produced water, and the materials options available.  The most difficult area is mixing produced water with raw sea water, and this was shown to cause some very corrosive mixtures, particularly when H2S was present.  The materials options available were outlined, as were the areas where there is a lack of data.  Cooling of the produced water prior to mixing with sea water is an option for reducing aggresivity prior to injection.  This has been adopted by the Statoil Nome project, which is using superduplex stainless steel.  An alternative is to have separate injection lines for raw water and produced water. 

"The RCP method for prevention of local corrosion on stainless steels in saline water piping systems", Mr Craig Donald, CorrOcean Ltd 

Some local corrosion failures have been experiences with highly alloyed stainless steels in chlorinated seawater piping systems used in oil and gas production.  The present paper presents the RCP method - Resistor controlled Cathodic Protection - as a means to avoid such corrosion problems in a simple and economic way.  The paper outlines the principles of the method and a more detailed discussion for the case of 6Mo stainless steels in chlorinated seawater.  The discussion comprises the protection potential, the current density requirements, the resistor control and the anode design.  Example calculations of the CP design including anode size, spacing and lifetime are presented.  Other applications are also briefly discussed. 

3   "Some corrosion mechanisms of tubes and pipes", Mr Ritchie Brown, BAeSEMA 

When inspecting heat exchanger tubes it is important to know the potential mechanisms of failure, their morphology and the methods available for inspection.  The aim of this is to ensure defects can be rectified during planned maintenance periods thus avoiding expensive unplanned shutdowns. Often a successful maintenance schedule is dependant on the customer knowing the fluids in the heat exchanger and the effect these have on the tube material.  Armed with this information the NDE specialist can advise the most suitable inspection technique. 

The presentation reviewed thirteen potential corrosion and cracking mechanisms with photographs showing examples of the morphology of the defects produced and the way these can vary depending on material selection and the environment.  From a range of corrosion mechanisms, under flowing and static conditions, the resulting defects can be on internal and external surface and can range from general wall thinning to isolated pitting.  The introduction of stresses can lead to axial and circumferential linear defects as a result of stress corrosion cracking and corrosion fatigue.  Vibrations, particularly between heat exchanger tubes and tube support plates, can also result in fretting damage. 

4    "Welding techniques for high alloy austenitic stainless steels", Dr Trevor G Gooch, TWI 

Factors controlling corrosion resistance of weldments in high alloy austenitic stainless steel were described, with emphasis on microsegregation, intermetallic phase precipitation and nitrogen loss from the molten pool.  The application was considered of a range of welding processes, both fusion and solid state. 

Autogenous fusion weldments have corrosion resistance below that of the parent, but low arc energy, high travel speed and use of N2-bearing shielding gas were recommended for best properties.  Conventional fusion welding practice is to use an overalloyed nickel-base filler metal to avoid preferential weld metal corrosion, and attention was given to the effects of consumable composition and level of weldpool dilution by base steel.  With non-matching consumables, overall joint corrosion resistance may be limited by the presence of a fusion boundary unmixed zone: better performance may be obtained using solid state friction welding, given appropriate component geometry. 

Overall, the effects of welding on superaustenitic steels were covered, and the materials have given excellent service in welded fabrications.  The presentation summarised recommendations on preferred welding procedure.

Technical presentations February 1996

1  "Seawater and firewater systems", Dr Mike Swidzinski, Phillips Petroleum Co.

The principal uses of seawater for offshore installations was considered with specific reference to the selection of materials for seawater handling, pumping and distribution.

Key considerations influencing material selection for seawater duty were addressed - issues such as galvanic compatibility, marine growth fouling, chemical treatments, seawater velocity, crevice and pitting corrosion were discussed in the context of identifying the most effective materials for seawater and firewater duty.

Materials that are commonly considered for seawater distribution and firewater systems were discussed.  These included:

Carbon Steel, Galvanised Carbon Steel, Austenitic Stainless Steels, Duplex Stainless Steels, Copper Alloys, including Copper-Nickel, Titanium, Nickel Based Alloys and Fibre-Reinforced Materials

The performance and general offshore industry experience encountered with the use of these materials was debated in open forum.

No clear conclusions regarding material selection could be drawn.  Each of the materials considered was shown to be fully effective for given aspects of seawater service - similarly each material considered was found to have inherent installation or performance limitations which would not favour its application for certain duties.  Consequently, no one material appeared as clear favourite for all offshore seawater and firewater applications.

The issue of material selection for seawater applications still requires close scrutiny by the Materials and Corrosion Engineer.  The optimum balance between CAPEX and OPEX still appears to be offered by a hybridised materials selection strategy – relying on simpler and cheaper materials for less arduous duties - through to the more exotic and corrosion resistant materials for the manufacture of more sensitive and strategically important items where whole-life reliability is paramount. 

2 "Comparison of the corrosion properties of cast aluminium bronze with stainless steels", Mr Vin Calicut, Copper Development Association

Aluminium bronzes have a long and successful history of use in seawater, it is the standard material specified for ships' propellers and is preferred for seawater systems in submarines.  Many workers have studied the corrosion resistance of aluminium bronzes, others have studied ferrous materials.  Few workers have studied both simultaneously. 

This project has collated data comparing the properties of cast nickel aluminium bronze (NAB), in particular NES 747 Part 2, with cast standard and superaustenitic and duplex stainless steels and Ni-Resist for use in offshore sea water applications.  Properties compared are physical, mechanical and fabrication but the bulk of the work has related to the corrosion aspects of the materials. 

Corrosion properties compared are general corrosion, pitting, resistance to polluted sea water, crevice corrosion, erosion corrosion, cavitation, stress corrosion cracking, corrosion fatigue and galvanic corrosion.  An overall composite ranking for the corrosion resistance has been established showing the superduplex stainless steels to be the best followed by the superaustenitic alloys with NAB close behind in third place.  The standard duplex, Ni-Resist and standard austenitic stainless steels make up the six. 

Within this composite ranking NAB stands up well against superduplex alloys in terms of general corrosion, pitting, cavitation and corrosion fatigue.  A pitting resistance temperature indicator (CPT or PREN) is not relevant to aluminium bronze.  Its erosion corrosion, although not as good is reasonable; it is immune to chloride stress corrosion cracking.  With regard to other properties it has comparable strength to the austenitic materials and can, by heat treatment have properties comparable to the duplex alloys but this may be accompanied by a loss in corrosion resistance. 

The alloy has excellent heat transfer and electrical conductivity properties as well as good wear resistance and anti fouling properties.  Its weldability is considered comparable with superduplex stainless steels. NAB should not be used in polluted sea water containing sulphides. 

Overall, providing the price of cast nickel-aluminium bronze is significantly lower than cast superduplex or superaustenitic stainless steels, there are many applications where it can compete successfully, based on cost linked with corrosion properties.  Typical examples of these applications are rising mains for fire hydrants, pumps and valves, desalination equipment and sea water valves for submarine applications. 

From a technical point of view these marine applications would use the major strengths of NAB compared particularly with superduplex stainless steel. These are: 

3.  "Materials selection for corrosion control in desalination plant", Dr Trevor Hodgkiess, Glasgow University

Dr Hodgkiess provided an overview of corrosion problems and their control in desalination plant with emphasis on the role of materials selection together with an indication of current issues in this subject area. The talk was illustrated throughout by corrosion and materials selection case studies from desalination plant.  The two main seawater desalination processes are distillation and reverse osmosis and the emphasis in the presentation was on the former process in which corrosion problems are more widespread. 

The review commenced with a detailed description of corrosion in seawater/brine and the role of oxygen control was identified before turning to the historical and current strategies relating to materials selection.  This involves the widespread use of Cu/Ni alloys or stainless steel either in solid form or as a cladding on carbon-steel.  The behaviour of stainless steels in the high temperature/deoxygenated environments within a thermal desalination plant was discussed.  The range of materials available for heat transfer tubing was also reviewed.  The speaker then moved on to the topic of corrosion in the vapour systems.  This is currently a cause of major concern in this respect are vapour chemistry, venting design and materials selection. Vapour space corrosion can involve oxygen and carbon dioxide from the normal seawater feed and can be further exacerbated by the presence of chlorine, bromine, ammonia or hydrogen sulphide. 

In relation to reverse osmosis units, the main corrosion issue is crevice corrosion of the high-pressure pipework components which are generally constructed from stainless steel.  The role of stainless steel grade was discussed. Finally, corrosion and material selection issues associated with ancillary components such as pumps and pipes was summarised.

Technical presentations January 1996

"Development in materials technology for marine pumps", Mr Len Phillips, Weir Pumps.

Centrifugal pumps are widely used in marine environments for handling seawater.  Pumps vary in size and complexity, dependent on the desired application.  These can a range from a relatively small single stage pump at low head for general service to a high pressure multi-stage pump for seawater injection duties.  

A wide range of materials are employed. For pump casings, cast iron and cast steel are viable for seawater only where corrosion protection is applied.  Austenitic cast iron affords increased corrosion and erosion resistance and provides galvanic protection to more noble pump internals. Copper based alloys such as gunmetals are also employed for pump casings, whilst nickel aluminium bronze provides a stronger, more corrosion resistant alloy where required.  

Stainless steels have seen major developments.  Although very popular for many years in seawater applications, 316 austenitic stainless steel has relatively poor crevice corrosion resistance and only modest strength. The development of duplex stainless steels has provided alloys with excellent resistance to crevice attack and stress corrosion cracking at high temperatures. Their increased strength allows the possibility of reduced cross sections and hence weight saving.  

For impellers, impingement and cavitation erosion resistance are most important.  A similar range of materials as that used for casings can be used for impellers.  Maximum performance will be obtained from the duplex stainless steels.  

The wear rings must possess good corrosion/erosion resistance and be mutually compatible.  Where suspended solids are present, hard particle erosion resistance is also required.  Austenitic cast iron, bronzes and stainless steels are all employed.  For more aggressive environments, one or both rings may be coated. Examples include stellite weld overlay, plasma spray CrO and HVOF tungsten carbide.  Solid materials such as sintered carbides and ceramics have also been used to combat excessive sand erosion.  

Possible future developments may include more corrosion resistant stainless steels and nickel based alloys and the increased use of titanium.  Where solids are present, the use of hard coatings and solid ceramics/hard metals may be more widespread.  

 2  "Performance of marine materials under erosive flow conditions", Dr Robert Wood, Southampton University.

This talk highlights the importance of erosion as a wear process and its affect on marine equipment, should it be ignored.  The main causes of erosion are introduced and discussed; namely where flows induce solid particle impingement, liquid droplet impingement and cavitation. The parameters which influence slurry erosion arc introduced and key parameters which must be controlled in any experimental approach identified.  Solid particle impingement results are presented for a wide range of marine materials and advanced materials/coatings obtained using a slurry jet erosion facility.  The potential of the ultra hard coatings for erosion resistant applications is noted.  The difference in erosion mechanisms for ductile and brittle materials are also discussed.  The influence of jet impingement angle and kinetic energy (Ek) on erosion rates are explored. Erosion maps for ductile and brittle materials based on kinetic energy terms, Ekv0.5 and Ek are presented as a useful marine materials selection tool.  Hydrodynamic cavitation erosion mechanisms are discussed and the resistance of marine materials to such damage mechanisms are reviewed. The ranking of such materials under cavitation erosion conditions are compared with those obtained under slurry erosion conditions and the differences discussed.  The importance of studying the performance of materials under realistic field conditions are highlighted by exploring the synergistic effects between erosion and corrosion. Current research projects in the area of surface engineering for marine applications are explained as an indication of possible future developments and use of advanced coatings.

"Structural Adhesives", Mr Alan Hunter, Altra Consultants Ltd.

This presentation addresses the rationale for the use of structural adhesives in marine environments.  A summary of Altra experience to date is given including both offshore and onshore usage.  Detailed discussion of outstanding issues is covered.

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